ISSN 1119-4618
 
2020, Vol: 20, Issue: 3
20/3Current Issue Online First Archive Aims and Scope Abstracting & Indexing Most Accessed Articles Most Downloaded Articles Most Cited Articles

Original Research 


Preparation of a High Siliceous ZSM-5 from Renewable Silica Source

Suleiman Yunusa, Mustapha Yusuf, Abdulkarim salawu Ahmed, Solomon Gajere Bawa, Maryam Abubakar.

Abstract
In this study, a highly siliceous ZSM-5 zeolite of elemental silicon to aluminium ratio of 365 was synthesized using rice husk ash (RHA) as a renewable source. The RHA was used to produce silica sol which, with the organic template tetrapropyl ammonium bromide (TPABr) as the structure directing agent went through hydrothermal reaction at low temperature and under atmospheric pressure in alkaline medium to form ZSM-5. The synthesized ZSM-5 was characterized using a variety of analytical techniques, including X-ray diffraction (XRD), Fourier transformation infrared spectroscopy (FT-IR), scanning electron microscopy (SEM) N2 adsorption and X-ray fluorescence (XRF) The specific surface area (SSA) was measured by the Brunauer, Emmet and Teller (BET) BET, Langmuir, and DFT methods. Furthermore, the pore volume and pore sizes were determined using Horvath-Kawazoe (H-K), Saito Foley (S-F) and Dubinin–Radushkevich (DR) and Density Functional Theory (DFT) methods and the results of these analysis compared well with the referenced ZSM-5.

Key words: ZSM-5; low temperature; RHA; Density Functional Theory; Horvath-Kawazoe; Saito Foley


 
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How to Cite this Article
Pubmed Style

Yunusa S, Yusuf M, Ahmed As, Bawa SG, Abubakar M, . Preparation of a High Siliceous ZSM-5 from Renewable Silica Source. JPAS. 2019; 17(1): 35-40. doi:10.5455/sf.27494

Web Style

Yunusa S, Yusuf M, Ahmed As, Bawa SG, Abubakar M, . Preparation of a High Siliceous ZSM-5 from Renewable Silica Source. http://www.atbuscienceforum.com/?mno=27494 [Access: March 21, 2021]. doi:10.5455/sf.27494

AMA (American Medical Association) Style

Yunusa S, Yusuf M, Ahmed As, Bawa SG, Abubakar M, . Preparation of a High Siliceous ZSM-5 from Renewable Silica Source. JPAS. 2019; 17(1): 35-40. doi:10.5455/sf.27494


Vancouver/ICMJE Style

Yunusa S, Yusuf M, Ahmed As, Bawa SG, Abubakar M, . Preparation of a High Siliceous ZSM-5 from Renewable Silica Source. JPAS. (2019), [cited March 21, 2021]; 17(1): 35-40. doi:10.5455/sf.27494


Harvard Style

Yunusa, S., Yusuf, M., Ahmed, A. s., Bawa, S. G., Abubakar, M. & (2019) Preparation of a High Siliceous ZSM-5 from Renewable Silica Source. JPAS, 17 (1), 35-40. doi:10.5455/sf.27494


Turabian Style

Yunusa, Suleiman, Mustapha Yusuf, Abdulkarim salawu Ahmed, Solomon Gajere Bawa, Maryam Abubakar, and . 2019. Preparation of a High Siliceous ZSM-5 from Renewable Silica Source. Science Forum (Journal of Pure and Applied Sciences), 17 (1), 35-40. doi:10.5455/sf.27494


Chicago Style

Yunusa, Suleiman, Mustapha Yusuf, Abdulkarim salawu Ahmed, Solomon Gajere Bawa, Maryam Abubakar, and . "Preparation of a High Siliceous ZSM-5 from Renewable Silica Source." Science Forum (Journal of Pure and Applied Sciences) 17 (2019), 35-40. doi:10.5455/sf.27494


MLA (The Modern Language Association) Style

Yunusa, Suleiman, Mustapha Yusuf, Abdulkarim salawu Ahmed, Solomon Gajere Bawa, Maryam Abubakar, and . "Preparation of a High Siliceous ZSM-5 from Renewable Silica Source." Science Forum (Journal of Pure and Applied Sciences) 17.1 (2019), 35-40. Print. doi:10.5455/sf.27494


APA (American Psychological Association) Style

Yunusa, S., Yusuf, M., Ahmed, A. s., Bawa, S. G., Abubakar, M. & (2019) Preparation of a High Siliceous ZSM-5 from Renewable Silica Source. Science Forum (Journal of Pure and Applied Sciences), 17 (1), 35-40. doi:10.5455/sf.27494


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